Remediation of Nickel from Crude Oil Obtained from Bomu Oil Field Using Cassava Waste Water Starch Stabilized Magnetic Nanoparticles

Joshua L. Konne, Kenneth Opara

Abstract


Starch Stabilized Magnetic Nanoparticles (SSMNPs) were prepared by reacting 4.4 g of FeCl3.6H2O with 1.98 g of FeCl2.4H2O in 61 mL of 0, 0.025, 0.5, 0.1 and 0.5% w/v of cassava waste water starch solution. Deionised water (0% w/v) was used as the control. Powder X-ray diffraction analysis of the first four samples confirmed that all the samples contained magnetite nanoparticles with estimated sizes of 16.99, 15.73, 11.48 and 17.73 nm respectively. The SSMNPs were then applied in the removal of nickel ions from crude oil obtained from Bomu oil field. The samples were divided into batches A and B. Both samples were shaken for 3.3 h but only batch A was centrifuged before analysis. 0.2 mL of each sample was siphoned and dissolved in n-hexane for analysis. The results obtained showed that the sample with the least starch concentration (15.73 nm) recorded the best performance in both cases with 56 and 93% of Ni (II) complexes removal respectively. All measurements were done using a UV-VIS spectrophotometer set at ?max of 400 nm predetermined from a scan of Ni (II) ions solution.


Full Text: PDF DOI: 10.5539/eer.v4n1p25

Refbacks

  • There are currently no refbacks.


Creative Commons License
This work is licensed under a Creative Commons Attribution 3.0 License.

Energy and Environment Research   ISSN 1927-0569 (Print)   ISSN 1927-0577 (Online)
Copyright © Canadian Center of Science and Education

To make sure that you can receive messages from us, please add the 'ccsenet.org' domain to your e-mail 'safe list'. If you do not receive e-mail in your 'inbox', check your 'bulk mail' or 'junk mail' folders.